Hybrid titration method
Easy factor determination by “Electrolytic Factor Measurement System”
Unique integrated “Hybrid titration cell” of both “Volumetric titration method” & “Coulometric titration method”
PRODUCT
Hybrid Karl Fischer Moisture Titrator
MKH-710M
Features
・Automatic sample injection
Hybrid titration method automatically switches the measurement methods of volumetric and coulometric according to the water content of the sample.
You can accurately and seamlessly measure samples without concern for the sample moisture content, as the instrument is capable of measuring trace or much larger quantities.
・No need to inject pure water Fully automatic factor measurement
Our unique “Electrolytic Factor Measurement System” carries out factor measurement automatically.
Just the press of a button enables factor measurement, which alleviates the need for
the tedious weighing or measuring of pure water.
・Single instrument and a single titration cell allow utilization of Volumetric/Coulometric/Hybrid Titration Methods.
Just one instrument with one titration cell is needed to perform volumetric, coulometric, and hybrid easurements.
With high operability for the volumetric method, the requisite sealability for the coulometric method has also been realized.
Integrated functionality greatly contributes to a ompact installation and low maintenance requirements.
- Original Functionality! World'first! "Hybrid titration method"
According to "Hybrid titration method", even if the water content of the sample is high, it can be carried out with high-speed & high-precision measurement.
- Original Functionality! World'first! Easy factor determination by "Electrolytic Factor Measurement System"
According to "Hybrid titration method", even if the water content of the sample is high, it can be carried out with high-speed & high-precision measurement.
- Unique integrated "Hybrid titration cell" of both "Volumetric titration method" & "Coulometric titration method"
While ensuring the seal, making the titration cell and titration cell stopper separate, it improves the convenience for usage.
- Titrant Information is stored in an IC chip in the burette unit (Smart burette)
- New burette unit
- Up to 4 simultaneous measurements (Simultaneous titrations)
- Can be connected to AT-710B potentiometric titrators ,MKV-710B volumetric Karl Fischer moisture titrators MKC-710B Coulometric Karl Fischer moisture titrators
- The main control unit and a titrator are separately located by wireless (Bluetooth(R))
- Large color TFT-LCD with a touch panel (8.4-inch)
- Two different user levels and permissions
- Measurement results are converted to PDF and can be stored in a USB flash drive
- Navigation function of Karl Fischer reagent replacement
- Automatic solvent change unit is included
Specification
Type | Hybrid Karl Fischer Moisture Titrator |
---|---|
Model | MKH-710M |
Coulometric titration | Measuring method : Karl Fischer Coulometric titration Measuring range : Water content : 1μg to 300mg H2O Bromine index : 8μg to 300mg Br Precision : RSD : less than 0.3% (n=10)(for measurements of 1mgH2O) Display resolution : 0.1μg |
Volumetric titration | Measuring method : Karl Fischer Volumetric titration Measuring range : Water content : 100μg - 500mg H2O(depends on KF reagent factor) Concentration : 1ppm - 100% H2O Burette precision : Volume : 10mL Discharge precision : ±0.015mL Repeatability : ±0.005mL |
Hybrid titration | Measuring method : Karl Fischer Coulometric titration Karl Fischer Volumetric titration Measuring range : Water content : 1μg - 500mg H2O Precision : RSD : less than 0.3% (n=10) (for measurements of 10mgH2O) (Karl Fischer reagent factor 3mg/mL) Display resolution : 0.1μg |
Factor measurement of reagent by electrolysis | Measuring method : Factor measurement of reagent by electrolysis Measuring range : KF reagent : Reagent factor from 1 to 5 (With the provisions of dose volume) Precision : RSD : less than 1.0% (n=3) (Dose volume 0.5mL, Reagent factor 3mg/mL) |
Method | 120 |
Key operation | Touch panel |
Displays | 8.4-inch color LCD 800 x 600 dots English / Japanese / Mandarin Chinese / Korean Simultaneous 4-channel display (Can also display Automatic Potentiometric Titrator simultaneously) |
Extensibility | Measuring instrument : Automatic Potentiometric Titrator (AT-710) , Karl Fischer Moisture Titrator (MKV-710/MKC-710/MKH-710) Three of these instruments can be added. |
Data storage | 500 samples |
GLP conformance | Registration of operator / User group administration Titrant : Reminder of factor measurement date / Alarm to indicate remaining reagent / Reminder of piston replacement date / Reminder of reagent replacement date / History of factor measurement / Reminder of expiration Check performance : Reminder of scheduled check date / Record of check results Management of conduction time : Display of operating time |
External I/O | RS-232C port x4 : for Dot matrix printer , Electronic balance , Data Capture Software (SOFT-CAP) , Multiple sample chager , Evaporator USB ×1 : for USB flash drive , A4 printer , Thermal printer , Keyboard , Barcode reader , Foot switch , USB HUB SS-BUS : Automatic piston burette : Can control max 2 burette drives (Including two built-in burette drives) LAN ×1 : for Personal computer (PC) |
Power Supply | Main unit: DC24V(Main unit), AC100-240V±10%, 50/60Hz(AC adapter) Printer: DC7V(Main unit), AC100V±10%, 50/60Hz(AC adapter) |
Power Consumption | Main unit: Approx. 30W, Printer: Approx. 7W |
Dimensions (Excluding tube) |
Touch panel controller: 225(W)×190(D)×42(H)mm Titration unit: 141(W)×292(D)×377(H)mm Stirrer/ Cell: 107(W)×206(D)×364(H)mm Solvent change unit: 240(W)×140(D)×400(H)mm Printer: 106(W)×180(D)×88(H)mm |
Weight | Touch panel controller: Approx. 1.5kg Titration unit: Approx. 4kg Stirrer/ Cell: Approx. 2kg Solvent change unit: Approx. 0.6kg Printer: Approx. 0.4kg |
Burette unit EBU FCC Part15 SubpartC FCC ID : 2ABSVEBU01
Standards
ASTM D1123 Standard Test Methods for Water in Engine Coolant Concentrate by the Karl Fischer Reagent Method
ASTM D1364 Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
ASTM D1533 Standard Test Method for Water in Insulating Liquids by Coulometric Karl Fischer Titration
ASTM D3401 Standard Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
ASTM D4377 Standard Test Method for Water in Crude Oils by Potentiometric Karl Fischer Titration
ASTM D4672 Standard Test Method for Polyurethane Raw Materials: Determination of Water Content of Polyols
ASTM D4928 Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
ASTM D5460 Standard Test Method for Rubber Compounding Materials—Water in Rubber Additives
ASTM D6304 Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration
ASTM D6869 Standard Test Method for Coulometric and Volumetric Determination of Moisture in Plastics Using the Karl Fischer Reaction (the Reaction of Iodine with Water)
ASTM E1064 Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
ASTM E203 Standard Test Method for Water Using Volumetric Karl Fischer Titration
European Pharmacopoeia / 2.5.12. WATER: SEMI-MICRO DETERMINATION
European Pharmacopoeia / 2.5.32. WATER: MICRO DETERMINATION
ISO 10101-3 Natural gas -- Determination of water by the Karl Fischer method -- Part 3: Coulometric procedure
ISO 12937 Petroleum products -- Determination of water -- Coulometric Karl Fischer titration method
ISO 14897 Plastics -- Polyols for use in the production of polyurethane -- Determination of water content
ISO 15512 Plastics -- Determination of water content
ISO 7335 Iron ores -- Determination of combined water content -- Karl Fischer titrimetric method
ISO 760 Determination of water -- Karl Fischer method (General method)
ISO 8534 Animal and vegetable fats and oils — Determination of water content — Karl Fischer method (pyridine free)
JIS C2101 Testing methods of electrical insulating oils
JIS K0068 Test methods for water content of chemical products
JIS K0113 General rules for methods of potentiometric, amperometric, coulometric, and Karl Fischer titrations
JIS K1557-2 Plastics -- Polyols for use in the production of polyurethane -- Part 2: Determination of water content
JIS K2275-2 Crude petroleum and petroleum products -- Determination of water -- Part 2: Potentiometric Karl Fischer titration method
JIS K2275-3 Crude petroleum and petroleum products -- Determination of water -- Part 3: Coulometric Karl Fischer titration method
JIS M8211 Iron ores -- Method for determination of combined water content
JIS M8250 Iron ores -- Determination of hygroscopic moisture in analytical samples -- Gravimetric, Karl Fischer titration and mass-loss methods
United States Pharmacopeia–National Formulary / 38 <921> WATER: DETERMINATION
Software
Option
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KEM Aqua Karl Fischer Reagents
“KEMAQUA Series"Karl Fischer Reagent “KEMAQUA Series" is a reagent made by Kyoto Electronics Manufacturing for use with Karl Fischer Moisture titrator. It is available for a wide range of samples.
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Evaporator
ADP-611Drying oven for moisture measurement on chip, particulate or powder samples such as plastic pellets
Maximum set temperature : 300℃ -
Evaporator for High Temperature
ADP-512SThis oven evaporates moisture in ores, metallic powder, ceramics and other solids and powder materials by high heat (maximum: 1000℃) for measurement of water content connected to Karl Fischer moisture titrator.
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Evaporator for Ores
ADP-512This oven is designed to use with KEM Karl Fischer moisture titrator for measurement of combined water in iron ores according to JIS M8211 Iron Ores – Method for Determination of Combined Water Content.
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Evaporator for Oil Samples
ADP-513This unit evaporates moisture of samples dissolved in a heated base oil.
This unit is primarily used for moisture measurements in lubricant oil, grease, tar products, paints and other viscous liquids. -
Heat Extractor for Sugar Samples
ADP-344The ideal solution sugary samples: This mantel heater for volumetric Karl Fischer titration cells ensures the complete extraction of the moisture content of samples like chocolates, caramels and other samples containing sugars.
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Multiple Sample Changer for Coulometric Karl Fischer Moisture Titrators
CHK-501Multiple sample evaporator for Coulometric Karl Fischer Moisture Titrators, suitable for the continuous measurement of up to 24 samples.
The heating temperature can be set for each sample individually, different kinds of sample can thus be measured automatically one after the other. An auto power off function after measurement ensures safe operation. -
Sampler
Sampler
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Titration Vessel
Titration Vessel
Catalog
■General-Catalog.pdf
■Hybrid Karl Fischer Moisture Titrator MKH-710M.pdf